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HRID543385

反应详情

EQUATION

反应方程式

HRID 543385 的结构方程式

REACTANTS

反应物

2
结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：COc1ccc(C(C)(C)C)cc1S(N)(=O)=O
HCID10933694

ST50778292

C11H17NO3S

PRODUCTS

生成物

1
结构：COc1ccc(C(C)(C)C)cc1S(=O)(=O)N=CN(C)C
HCID54498328

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

4.68 g (0.02 mol) of 3-(1,1-dimethylethyl)-6-methoxybenzenesulfonamide are dissolved in 50 ml of dimethylformamide, and 2.5 g (0.022 mol) of dimethylformamide dimethyl acetal are added. The mixture is left at room temperature for 30 minutes, then poured onto ice-water and filtered with suction.

WORKUP

后处理

  1. additionpoured onto ice-water
  2. filtrationfiltered with suction