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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 543485Generated: October 30, 2026

Sodium Hydroxide → HCID 178513314, compound

https://huagongshe.com/reaction/543485

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 178523923HCID 178523923—
SolventWater ethanolHCID 19096565—
ProductHCID 178513314HCID 17851331487.5%

Reaction Steps

38.5 g 1-(2,6-dichlorophenyl)-2-benzoyl-3-tetrahydropyranyloxyguanidine are heated to a boil with 900 ml 5% NaOH (in a mixture water/ethanol 1:1) for 2 hours. After cooling, 25.1 g 1-(2,6-dichlorophenyl)-2-tetrahydropyranyloxyguanidine having a melting point of 178°-180° C. is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04446142
Source datasetuspto-grants-1984_05
ORD IDord-85e6a2c08c844689960b1ce4947357e5
Source noteuspto-grants-1984_05