HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → HCID 86739390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | 1,3-Benzodioxole-5-ethanamine | HCID 73874 | — |
| Product | HCID 86739390 | HCID 86739390 | 43.8% |
Reaction Steps
A mixture of 16.5 g of 3,4-methylenedioxyphenylethylamine and 40.5 g of ethyl acrylate is refluxed for 24 hours over an oil bath. After cooling, the mixture is concentrated under reduced pressure to distill away excess ethyl acrylate. 16 g of N,N-bis (β-ethoxycarbonylethyl)-3,4-methylenedioxyphenylethylamine is obtained as the residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04446141 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-e0331274ca7348719983e6ee7b2abe9e |
| Source note | uspto-grants-1984_05 |