Ethyl Acrylate → HCID 86739390, compound

HRID 543489Notes

Reaction equation

HRID 543489 reaction equation
[CH2:1]1[O:9][C:8]2[CH:7]=[CH:6][C:5]([CH2:10][CH2:11][NH2:12])=[CH:4][C:3]=2[O:2]1.[C:13]([O:17][CH2:18][CH3:19])(=[O:16])[CH:14]=[CH2:15]>>[CH2:18]([O:17][C:13]([CH2:14][CH2:15][N:12]([CH2:11][CH2:10][C:5]1[CH:6]=[CH:7][C:8]2[O:9][CH2:1][O:2][C:3]=2[CH:4]=1)[CH2:15][CH2:14][C:13]([O:17][CH2:18][CH3:19])=[O:16])=[O:16])[CH3:19]

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 738741,3-Benzodioxole-5-ethanamine

Product 1

HCID 86739390HCID 86739390, compoundYield 43.8%

Procedure

A mixture of 16.5 g of 3,4-methylenedioxyphenylethylamine and 40.5 g of ethyl acrylate is refluxed for 24 hours over an oil bath. After cooling, the mixture is concentrated under reduced pressure to distill away excess ethyl acrylate. 16 g of N,N-bis (β-ethoxycarbonylethyl)-3,4-methylenedioxyphenylethylamine is obtained as the residue.

Workup

  1. temperatureis refluxed for 24 hours over an oil bath
  2. temperatureAfter cooling
  3. concentrationthe mixture is concentrated under reduced pressure
  4. distillationto distill away excess ethyl acrylate

Sources & evidence

ORD record
ord-e0331274ca7348719983e6ee7b2abe9e
Source dataset
uspto-grants-1984_05
Patent number
US04446141

Reaction notes

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