HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131713501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 20461679 | HCID 20461679 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131713501 | HCID 131713501 | — |
Reaction Steps
Methyl 2-fluoromethyl-2,5-di(tert-butoxycarbonylamino)-4-methylene pentanoate (0.72 g) obtained in Step C above is treated with dry ether saturated with HCl gas. After stirring overnight the title compound is collected (0.38 g, 78%). Recrystallisation from isopropanol/ethyl acetate gives the pure product yield 300 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04446151 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-42643367b62d441a9b55c6223cb4a339 |
| Source note | uspto-grants-1984_05 |