Potassium Persulfate → Butyl Acrylate

HRID 543524Notes

Reaction equation

HRID 543524 reaction equation
C([C:9]([CH2:21][CH2:22]CCCCCC)([C:18]([O-:20])=O)C(S(O)(=O)=O)C([O-])=O)CCCCCCC.[Na+].[Na+].S(OOS([O-])(=O)=O)([O-])(=O)=O.[K+].[K+]>O>[C:18]([O:20][CH2:18][CH2:9][CH2:21][CH3:22])(=[O:20])[CH:9]=[CH2:21]

Participants

4

Reactant 2

HCID 24412Potassium PersulfateHCID 21924627HCID 21924627, compound

Product 1

HCID 8846Butyl Acrylate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
65 °C

Procedure

98 Parts of butyl acrylate and 2 parts of tricyclodecenyl acrylate are polymerized in 154 parts of water containing 2 parts of sodium dioctylsulfosuccinate (70% strength) as emulsifier and 0.5 part of potassium persulfate by stirring for 3 hours at 65° C. A 40% strength dispersion is obtained, the mean particle size of the latex being about 0.1 μm.

Workup

  1. customA 40% strength dispersion is obtained

Sources & evidence

ORD record
ord-a94a7621c1de40ef920f6e958629c4af
Source dataset
uspto-grants-1984_05
Patent number
US04446277

Reaction notes

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