HuagongsheHuagongshe Chemistry Print Report · For research reference only
6a,7,8,9-tetrahydropyrido[3,2-e]pyrrolo[1,2-a]pyrazin-6(5H)-one → 5,6,6a,7,8,9-Hexahydropyrido[3,2-e]pyrrolo[1,2-a]pyrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6a,7,8,9-tetrahydropyrido[3,2-e]pyrrolo[1,2-a]pyrazin-6(5H)-one | HCID 2766187 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 5,6,6a,7,8,9-Hexahydropyrido[3,2-e]pyrrolo[1,2-a]pyrazine | HCID 13342094 | — |
Reaction Steps
Following the procedure of Example 3, 6a,7,8,9-tetrahydropyrido[3,2-e]pyrrolo[1,2-a]pyrazin-6(5H)-one is reduced with lithium aluminum hydride to afford the title compound as the hydrochloride salt, m.p. 198°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04446323 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-4fce1c8cdd34408a9a15a6f467e743cb |
| Source note | uspto-grants-1984_05 |