Hydrogen iodide → HCID 20200300, compound

HRID 543639Notes

Reaction equation

HRID 543639 reaction equation
C[O:2][C:3]1[CH:29]=[N:28][C:6]2[N:7]([CH2:22][CH2:23][CH2:24][N:25]([CH3:27])[CH3:26])[C:8]3[CH:21]=[CH:20][CH:19]=[CH:18][C:9]=3[C:10]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[N:11][C:5]=2[CH:4]=1.I>C(O)(=O)C>[OH:2][C:3]1[CH:29]=[N:28][C:6]2[N:7]([CH2:22][CH2:23][CH2:24][N:25]([CH3:26])[CH3:27])[C:8]3[CH:21]=[CH:20][CH:19]=[CH:18][C:9]=3[C:10]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[N:11][C:5]=2[CH:4]=1

Participants

4

Reactant 2

HCID 24841Hydrogen iodideHCID 20200319HCID 20200319, compound

Product 1

HCID 20200300HCID 20200300, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The title compound is prepared by reacting 3-methoxy-N,N-dimethyl-6-phenyl-11H-pyrido[2,3-b][1,4]benzodiazepine-11-propanamine with hydrogen iodide and glacial acetic acid.

Sources & evidence

ORD record
ord-a42b4808aa5f490f8ca037cc9d134350
Source dataset
uspto-grants-1984_05
Patent number
US04447361

Reaction notes

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