HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178482377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178469832 | HCID 178469832 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178482377 | HCID 178482377 | — |
Reaction Steps
2-Methylamino-5-ethoxycarbonyl-4-hydroxypyrimidine (360 mg 1.9 mmol) was hydrolysed in boiling water (10 ml) with NaOH (0.19 g, 4.7 mmol) for 2 h. Cooling and acidification to pH 2 yielded the named product as a precipitate (261 mg, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04447422 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-b4ae96302c0f45ac81125c444da4504e |
| Source note | uspto-grants-1984_05 |