HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanamine, acetate → HCID 178456849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanamine, acetate | HCID 12203663 | — |
| Reactant | HCID 178418871 | HCID 178418871 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178456849 | HCID 178456849 | — |
Reaction Steps
2-Methylthio-5-ethoxycarbonyl-4-hydroxypyrimidine (2 mmol, 428 mg) was heated on an oil bath at 160° C. with n-propylamine acetate (1 ml) for 1 hour. The semi solid was cooled and then treated with 50 ml boiling water, and the solid product was filtered off (yield 400 mg, 88%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04447422 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-29a8e092abdd40efa21bc881d67aaf27 |
| Source note | uspto-grants-1984_05 |