HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 12807846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 12807845 | HCID 12807845 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 12807846 | HCID 12807846 | — |
Reaction Steps
In a similar manner to that described in Example 4 7-chloro-1-methyl-3-methylthiomethyl-4-quinolone was oxidised with 3-chloroperbenzoic acid to give the novel 7-chloro-1-methyl-3-methylsulphinylmethyl-4-quinolone m.p. 180°-181° (from dichloromethane:petroleum ether (b.p. 60°-80°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04447435 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-323d6cb615bb40cab563a26ca06c7c8e |
| Source note | uspto-grants-1984_05 |