Hydrochloric Acid → HCID 20459485, compound

HRID 544125Notes

Reaction equation

HRID 544125 reaction equation
[CH2:1]([N:8]([CH3:19])[CH2:9][CH2:10][NH:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:20]>C(OCC)C>[ClH:20].[ClH:20].[CH2:1]([N:8]([CH3:19])[CH2:9][CH2:10][NH:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18982043HCID 18982043, compound

Product 1

HCID 20459485HCID 20459485, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

6.15 g of N,N'-dibenzyl-N-methyl-ethylenediamine are dissolved in 60 ml of diethyl ether. Hydrogen chloride is then introduced while stirring and cooling (if necessary in an acetone/dry-ice bath) until a sample, dried on a clay plate, melts at 227°-229° C. The precipitated product is filtered with suction, washed with ether and dried to constant weight under reduced pressure (under 0.1 mbar). N,N'-dibenzyl-N-methyl-ethylenediamine dihydrochloride is obtained, m.p. 227°-229° C.

Workup

  1. temperaturecooling (if necessary in an acetone/dry-ice bath) until a sample
  2. customdried on a clay plate, melts at 227°-229° C
  3. filtrationThe precipitated product is filtered with suction
  4. washwashed with ether
  5. customdried to constant weight under reduced pressure (under 0.1 mbar)

Sources & evidence

ORD record
ord-8d6e106a5ff34d138c2c41f8abd2f26a
Source dataset
uspto-grants-1984_05
Patent number
US04448776

Reaction notes

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