反应详情

A mixture of 1.0 g 5-hydroxymethyl-3-methoxy-isoxazole and 10 g thionyl chloride was stirred at room temperature for 20 h. The excess thionylchloride was removed in vacuo, dissolved in toluene and the solvent evaporated. 1.0 g of an oil was obtained.

1. customThe excess thionylchloride was removed in vacuo
2. dissolutiondissolved in toluene
3. customthe solvent evaporated