HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 13326260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 13326259 | HCID 13326259 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13326260 | HCID 13326260 | — |
Reaction Steps
An excess of N-bromosuccinimide in acetic acid is added to 1-(2,4,6-trichloroanilino)-2,4-pyrimidinedione and the mixture is refluxed for 10 hours. It is cooled to RT and is then poured into ice and filtered to give 5-bromo-1-(2,4,6-trichloroanilino)-2,4-pyrimidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04448961 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-ba80c9f26a574143b84fd07f58ecaab7 |
| Source note | uspto-grants-1984_05 |