HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14234525, compound → HCID 70511443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14234525 | HCID 14234525 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 70511443 | HCID 70511443 | — |
Reaction Steps
A solution of 1-(tert-butyloxycarbonyl)-N-(3-phenylpropyl)-L-prolinamide (2.88 g.) in ethyl acetate-hydrogen chloride (3.9 N, 30 ml.) was stirred at room temperature for one half hour, then concentrated. A solution of the residue (2.80 g.) in ethyl acetate was concentrated, affording N-(3-phenylpropyl)-L-prolinamide hydrochloride as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04450155 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-f50268dad86d45c2b881b8f81fe1a37f |
| Source note | uspto-grants-1984_05 |