Aniline → HCID 20458931, compound

Participants

Reaction Steps

To 4.3 g (0.03 mole) of 4-chloro-5,6-dimethylpyrimidine were added 2.8 g (0.03 mole) of aniline; the mixture was then heated at 100°-150° C. for about 3 minutes. The reaction mixture quickly became a solution and soon produced a precipitate, which was collected by filtration and then recrystallised from ethanol to give 3.2 g(yield 40%) of the desired Compound No. 23, in the form of a colourless powder melting at 243°-245° C.

Provenance & Evidence