HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5-Dihydro-2-thiazolamine → HCID 178479725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5-Dihydro-2-thiazolamine | HCID 15689 | — |
| Reactant | Ethyl 7-chloro-4-oxo-1,4-dihydroquinoline-3-carboxylate | HCID 345422 | — |
| Product | HCID 178479725 | HCID 178479725 | — |
Reaction Steps
Using the procedure of Example 2, ethyl 7-chloro-4-hydroxy-3-quinoline-carboxylate and 2-amino-thiazoline were reacted at reflux for 48 hours and the product was crystallized from acetic acid to obtain N-(4,5-dihydro-thiazol-2-yl)-7-chloro-4-hydroxy-3-quinoline-carboxamide hydrochloride melting at >260° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04450166 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-c26c38fffa284a5ebb2ee5c624107b7f |
| Source note | uspto-grants-1984_05 |