HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanedithiol → HCID 88718880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanedithiol | HCID 8013 | — |
| Reactant | 1,1-Dichloro-2,2-diethoxyethane | HCID 12080 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 88718880 | HCID 88718880 | 126.4% |
Reaction Steps
In 100 ml of benzene, 9.4 g of dichloroacetaldehyde diethylacetal was reacted with 5.4 g of propane-1,3-dithiol. After distilling off the benzene/ethanol azeotrope at 68° C., there was obtained a yield of 10.2 g of the title compound, nD30 1.5850. The structure was supported by analytical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451280 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-057872ff02a54dda906ad8d5033d665b |
| Source note | uspto-grants-1984_05 |