HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 544534Generated: October 30, 2026
Methanesulfonic Acid → HCID 20458153, compound
https://huagongshe.com/reaction/544534
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | Diphenyl Ether | HCID 7583 | — |
| Reactant | Diphenyl sulfoxide | HCID 13679 | — |
| Product | HCID 20458153 | HCID 20458153 | 54.6% |
Reaction Steps
A mixture of 40.45 g pheny sulfoxide, 340.42 g of diphenyl ether and 192.20 g of methane sulfonic acid was heated at 100° C. for 68 hours. The disappearance of phenyl sulfoxide was monitored by gas chromatography. Workup substantially according to the method of Example 3 gave 49.24 g of diphenyl-4-phenoxyphenylsulfonium methane sulfonate (54.6 percent yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04451408 |
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| Source dataset | uspto-grants-1984_05 |
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| ORD ID | ord-e6164f7ca5e04c0ba21c53ed30b5ff75 |
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| Source note | uspto-grants-1984_05 |
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