HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1-propanol → HCID 178509295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1-propanol | HCID 12313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 5-amino-1H-1,2,4-triazole-3-thiol | HCID 178509296 | — |
| Product | HCID 178509295 | HCID 178509295 | 66.1% |
Reaction Steps
A mixture of 3-amino-5-mercapto-1,2,4-triazole (1.16 g.), 2 N aqueous sodium hydroxide (6 ml.) and 3-chloropropanol (1.1 g.) was heated at 90° for 1 hour and then cooled. The white solid which crystallised was collected to give 3-amino-5-(3-hydroxypropylthio)-1,2,4-triazole (1.15 g.), m.p. 136°-137°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451463 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-077fdaa1d40d4b75b40df01c3fa13dae |
| Source note | uspto-grants-1984_05 |