HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 53782809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | Cyanamide, [2-(methylthio)-4-pyrimidinyl]- | HCID 20458209 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53782809 | HCID 53782809 | — |
Reaction Steps
A mixture of 4-cyanoamino-2-methylthiopyrimidine (0.83 g.) and n-propylamine (0.6 ml.) was heated under reflux in acetonitrile (20 ml.) for 1 hour. The solvent was evaporated in vacuo and the residue suspended in dilute aqueous sodium hydroxide. The solid was collected, washed with water and dried to give 4-(2-propylguanidino)-2-methylthiopyrimidine, m.p. 177°-178°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451463 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-c91a9f7f7ff34155bef03e449cc34e15 |
| Source note | uspto-grants-1984_05 |