HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20202846, compound → HCID 20458260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20202846 | HCID 20202846 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20458260 | HCID 20458260 | — |
Reaction Steps
A stirred mixture of methyl 3-(4-amino-1,2,3-triazol-2-yl)benzoate (0.312 g.), lithium aluminium hydride (0.10 g.) and ether (50 ml.) was kept at room temperature for 1 hour. The excess of lithium aluminium hydride was destroyed with aqueous NaOH and the mixture was filtered. The filtrate was evaporated to give unpurified 4-amino-2-(3-hydroxymethylphenyl)-1,2,3-triazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451463 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-afec93e93eab4688962a0ec4d7acdda7 |
| Source note | uspto-grants-1984_05 |