HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromodiphenylmethane → HCID 20458406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromodiphenylmethane | HCID 236603 | — |
| Reactant | Fumarate | HCID 5460307 | — |
| Reactant | 3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonan-9-ol | HCID 12360832 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20458406 | HCID 20458406 | 50% |
Reaction Steps
10 g of 3,7-dimethyl-3,7-diazabicyclo[3.3.1]nonane-9-ol are reacted with 24.7 g of benzhydryl bromide as described in Example 1. The product is converted into its fumarate, the salt is dissolved in methanol, and precipitated with methylethyl-ketone. 3,7-Dimethyl-9-benzhydryloxy-3,7-diazabicyclo[3.3.1]nonane fumarate is obtained with a yield of 50%; m.p.: 200°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451473 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-68b15cd5e2294595a940f6ff25d322a7 |
| Source note | uspto-grants-1984_05 |