HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 20458410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 20458403 | HCID 20458403 | — |
| Product | HCID 20458410 | HCID 20458410 | 53.8% |
Reaction Steps
9.9 g of 3,7-diethyl-3,7-diazabicyclo[3.3.1]nonane-9-ol are reacted with 4-chloro-benzoyl chloride as described in Example 8 to obtain 3,7-diethyl-9-(4'-chloro-benzoyloxy)-3,7-diazabicyclo[3.3.1]nonane dihydrochloride monohydrate with a yield of 53.8%; m.p.: 116°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451473 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-a8512eaefd344afcb07ff8f963393b83 |
| Source note | uspto-grants-1984_05 |