1,6-Dibromohexane → 4-[(6-Bromohexyl)oxy]benzonitrile

HRID 544601Notes

Reaction equation

[K].[C:2]([C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1)#[N:3].[Br:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]Br>>[C:2]([C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][Br:11])=[CH:6][CH:5]=1)#[N:3]

Participants

Reactant 3

HCID 123681,6-Dibromohexane

HCID 130194-Cyanophenol

HCID 5462222Potassium

Product 1

HCID 134508844-[(6-Bromohexyl)oxy]benzonitrile

Procedure

The intermediate 6-(4-cyanophenoxy)hexyl bromide was prepared from the potassium salt of 4-cyanophenol and 1,6-dibromohexane.

Sources & evidence

ORD record: ord-0a1546c72aca43fc8500ae6892baef73
Source dataset: uspto-grants-1984_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04451476

Reaction notes

Loading…