HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → 3-(5-Bromopentyl)-5-methylisoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 3-(5-Hydroxypentyl)-5-methylisoxazole | HCID 13316977 | — |
| Product | 3-(5-Bromopentyl)-5-methylisoxazole | HCID 13316978 | 77% |
Reaction Steps
3-(5-Bromopentyl)-5-methylisoxazole was prepared by reacting 3-(5-hydroxypentyl)-5-methylisoxazole with bromine and triphenylphosphine according to the procedure of part (f) above, and was obtained in 77% yield as an oil, b.p. 140°-150° C.(0.05 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04451476 |
| Source dataset | uspto-grants-1984_05 |
| ORD ID | ord-fce2d7781be84cbf98c0333fd12b0113 |
| Source note | uspto-grants-1984_05 |