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A 0.6 g. amount of sodium metal is dissolved in 100 ml. of absolute ethanol, then 14.76 g. of m-chlorophenylhydrazine is added followed in 5 minutes by 12.92 g. of cinnamonitrile. The reaction mixture is refluxed for 6 hours, then cooled in an ice-bath. The precipitate formed is collected by filtration, then is dissolved in dichloromethane. This solution is passed through a short column of a hydrous magnesium silicate. The effluent is heated to reflux on a steam bath and hexane is added until a precipitate occurs. The product is collected, then is recrystallized from dichloromethane-hexane to give 7.55 g. of the product of the Example as salmon colored needles, m.p. 164°-165° C.

1. temperatureThe reaction mixture is refluxed for 6 hours
2. temperaturecooled in an ice-bath
3. customThe precipitate formed
4. filtrationis collected by filtration
5. dissolutionis dissolved in dichloromethane
6. temperatureThe effluent is heated
7. temperatureto reflux on a steam bath
8. additionhexane is added until a precipitate
9. customThe product is collected
10. customis recrystallized from dichloromethane-hexane
11. customto give 7.55 g