Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Solvent | Water | HCID 962 | — |
| Product | Nitrobenzene | HCID 7416 | 302.4% |
Reaction Steps
A solution of sodium hydroxide (7.1 g) in water (7.1 g) and benzyltriethylammonium chloride (0.4 g) was added to a mixture of 4-fluoronitrobenzene (14.1 g) and 1,1,7-trihydryl-F-heptanol (36 g). The whole was stirred and heated at about 60° C. for about 6 hours. The product was recrystallized from an ethanol/petroleum ether mixture to give 4-(1,1,7-trihydryl-F-hepyloxy) nitrobenzene (37.2 g), having a melting point of 51°-53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04451645 |
|---|
| Source dataset | uspto-grants-1984_05 |
|---|
| ORD ID | ord-9c5109867c2d436daa71fdf51c714d05 |
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| Source note | uspto-grants-1984_05 |
|---|
