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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 544839Generated: October 28, 2026

HCID 66631372, compound → HCID 66630811, compound

https://huagongshe.com/reaction/544839

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66631372HCID 66631372—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 66630811HCID 66630811100%

Reaction Steps

A mixture of 4-(5-nitro-pyrimidin-2-yl)-1,4-diaza-bicyclo[3.2.2]nonane (0.71 g, 2.85 mmol), palladium (0.25 g, 10% on activated carbon) and methanol (50 ml) was stirred under hydrogen for 10 min. The reaction-mixture was filtered through celite and was washed with ethanol (50 ml). The product was dried and evaporated. Yield 100%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07935695B2
Source datasetuspto-grants-2011_05
ORD IDord-c0d72b5517c04980ad3a1b527bdd1757
Source noteuspto-grants-2011_05