HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66631372, compound → HCID 66630811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66631372 | HCID 66631372 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66630811 | HCID 66630811 | 100% |
Reaction Steps
A mixture of 4-(5-nitro-pyrimidin-2-yl)-1,4-diaza-bicyclo[3.2.2]nonane (0.71 g, 2.85 mmol), palladium (0.25 g, 10% on activated carbon) and methanol (50 ml) was stirred under hydrogen for 10 min. The reaction-mixture was filtered through celite and was washed with ethanol (50 ml). The product was dried and evaporated. Yield 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935695B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-c0d72b5517c04980ad3a1b527bdd1757 |
| Source note | uspto-grants-2011_05 |