HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 24985575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 45429161 | HCID 45429161 | — |
| Product | HCID 24985575 | HCID 24985575 | 73% |
Reaction Steps
The title compound (Example 186) was prepared by reacting 3-(5-(4-chlorophenyl)thiophene-2-carboxamido)-4-methylbenzoic acid C with methylamine using the method described in Example 128 to afford a white solid in 73% yield. HPLC Ret. Time=3.51 min, LCMS [M+H]+ 385.08.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935696B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-c94a4516294c4ddcb676ab6693eaac5b |
| Source note | uspto-grants-2011_05 |