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HRID545011

反应详情

EQUATION

反应方程式

HRID 545011 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

结构：CN(C)C=C1CC(=O)Nc2ccc(Br)cc2C1=O
HCID66934668

未命名化合物

结构：COc1ccc(NC(=N)N)cc1OC
HCID178492306

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(Nc2ncc3c(n2)-c2cc(Br)ccc2NC(=O)C3)cc1OC
HCID59851156

未命名化合物

PROCEDURE

实验过程

In a manner similar to method I (NaHCO3 used instead of K2CO3), 7-bromo-4-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-k) and 1-(3,4-dimethoxyphenyl)-guanidine were converted to I-18 (74%): HRMS Calcd. for C20H17BrN4O3: 441.0562, Found 441.0548.