HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 178472262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 86616377 | HCID 86616377 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178472262 | HCID 178472262 | — |
Reaction Steps
The resultant product (600 mg) of (166-1) and thiourea (250 mg) were dissolved in ethanol (100 mL), and the mixture was heated under reflux for 48 hrs. The yellow solid precipitated in the reaction mixture was collected by filtration and washed with water and ethyl acetate to give the title compound (500 mg) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935700B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-0cce5a6b182f449ea59565a673321950 |
| Source note | uspto-grants-2011_05 |