HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-fluoro-2-methyl-4-nitro- → HCID 43373591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| Reactant | 4-Amino-1-methylpiperidine | HCID 2737531 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 43373591 | HCID 43373591 | — |
Reaction Steps
In the same manner as in Production Example 5-1 but using 1-methylpiperidine-4-amine in place of N-ethylpiperazine used in Production Example 5-1, using 2-fluoro-5-nitrotoluene in place of 2-fluoro-5-nitrobenzyl alcohol and using dimethylsulfoxide in place of N-methylpyrrolidone, 1.2 g of the entitled compound was obtained as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935708B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-0b4227f2eea6469186d685859530e664 |
| Source note | uspto-grants-2011_05 |