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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 545491Generated: October 29, 2026

Methanesulfonyl chloride → HCID 11486101, compound

https://huagongshe.com/reaction/545491

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonyl chlorideHCID 31297—
ReactantHCID 11473695HCID 11473695—
ProductHCID 11486101HCID 11486101—

Reaction Steps

The title compound was prepared in procedures similar to those described for the preparation of 6-[(acetyl-benzyl-amino)-methyl]-benzo[b]thiophene-2-carboxylic acid hydroxyamide. Methanesulfonyl chloride was used instead of acetic anhydride for the preparation of this title compound. 1H NMR (DMSO-d6, 200 MHz) δ 11.46 (brs, 1H), 9.29 (brs, 1H), 7.90-7.76 (m, 3H), 7.36-7.16 (m, 6H), 4.43 (s, 2H), 4.33 (s, 2H), 2.99 (s, 3H). MS (EI): cal'd 389.1 (M−H−), exp 389.2 (M−H−).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07935724B2
Source datasetuspto-grants-2011_05
ORD IDord-cee531546e9a429a83ba26bba457c134
Source noteuspto-grants-2011_05