HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Bromo-3-fluorophenyl)hydrazine → HCID 57431651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Bromo-3-fluorophenyl)hydrazine | HCID 12149225 | — |
| Reactant | 2-Methyl-N-(4-oxocyclohexyl)propanamide | HCID 21533994 | — |
| Product | HCID 57431651 | HCID 57431651 | — |
Reaction Steps
Prepare the title compounds by essentially following the procedure as described in Preparation 4 (Method 2) with (4-bromo-3-fluoro-phenyl)-hydrazine (Preparation 12) and N-(4-oxo-cyclohexyl)-isobutyramide, to obtain a tan solid containing a 65:35 mixture of isomers in 20% overall yield. MS (ES): m/z 353, 355 (M+H), 351, 353 (M−H); HPLC (Method A): Rt=2.22 min, (95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935722B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-2216c89422e34bb793a5269e0a1e6f7a |
| Source note | uspto-grants-2011_05 |