HRID545522

反应详情

EQUATION

反应方程式

HRID 545522 的结构方程式

PROCEDURE

实验过程

Prepare the tide compound by essentially following the procedure as described in Preparation 4 (Method 2) with 2-fluoro-4-bromophenylhydrazine (Preparation 14) and N-(4-oxo-cyclohexyl)-isobutyramide, to obtain the title compound as a tan foam in 32% yield. MS (ES): m/z 353, 355 (M+H), 351, 353(M−H); HPLC (Method A): Rt=2.34, (89%).

WORKUP

后处理

  1. customPrepare the tide compound