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HRID545526

反应详情

EQUATION

反应方程式

HRID 545526 的结构方程式

REACTANTS

反应物

2
结构：Fc1cccc(CBr)c1
HCID68007

Benzene, 1-(bromomethyl)-3-fluoro-

C7H6BrF

结构：CC(C)C(=O)NC1CCc2[nH]c3c(F)cc(Br)cc3c2C1
HCID57431654

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)C(=O)NC1CCc2c(c3cc(Br)cc(F)c3n2Cc2cccc(F)c2)C1
HCID59161271

未命名化合物

收率 36%

PROCEDURE

实验过程

Prepare the title compound by essentially following the procedure as described in Example 96 with N-(6-bromo-8-fluoro-2,3,4,9-tetrahydro-1H-carbazol-3-yl)-isobutyramide (Preparation 19) and 3-fluorobenzyl bromide, to obtain the title compound as a white solid in 36% yield. MS (ES): m/z 461,463 (M+1), 459, 461 (M−1); HPLC (Method A): Rt=4.60 (92%).