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HRID545571

反应详情

EQUATION

反应方程式

HRID 545571 的结构方程式

REACTANTS

反应物

2
结构：Fc1cccc(CBr)c1
HCID68007

Benzene, 1-(bromomethyl)-3-fluoro-

C7H6BrF

结构：N#Cc1ccc2[nH]c3c(c2c1)CC(NC(=O)C1CC1)CC3
HCID59161240

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1ccc2c(c1)c1c(n2Cc2cccc(F)c2)CCC(NC(=O)C2CC2)C1
HCID59161234

未命名化合物

PROCEDURE

实验过程

Prepare the title compound from cyclopropanecarboxylic acid(6-cyano-2,3,4,9-tetrahydro-1H-carbazol-3-yl)amide (3.00 g, 10.7 mmol) and 3-fluorobenzyl bromide (2.2 g, 11.8 mmol) by essentially following procedures as described in Example 1 to obtain 1.4 g (34%) of a beige solid. mp: 207-209° C.; MS (ES): m/z 388 (M+1); HPLC: Rt=2.28 min (100%).