Sodium Hydroxide → HCID 72234595, compound

Participants

Reaction Steps

Prepare the title compound from cyclopropanecarboxylic acid(6-formyl-2,3,4,9-tetrahydro-1H-carbazol-3-yl)-amide (Preparation 72) (6.50 g, 57.3 mmol) methoxylamine hydrochloride (4.81 g, 57.6 mmol) and sodium hydroxide (1.84 g, 46.0 mmol), by essentially following procedures as described in Example 202 to obtain 6.00 g (84%) of product. MS (ES): m/z 312 (M+1).

Provenance & Evidence