HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 14719547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 6-Methoxy-4-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydroisoquinoline | HCID 14719546 | — |
| Product | HCID 14719547 | HCID 14719547 | — |
Reaction Steps
To 790 mg of 6-methoxy-4-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydroisoquinoline, was added 16 ml of 48% hydrobromic acid, and the mixture was heated under reflux for 3 hours under an argon stream. The reaction solution was cooled, and precipitates which separated out were collected by filtration, giving 630 mg of 6-hydroxy-4-(3,4-dihydroxyphenyl)-1,2,3,4-tetrahydroisoquinoline hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05623074 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-a0f164230cc140298893bee2f8c9c1f3 |
| Source note | uspto-grants-1997_04 |