HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N'-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate → 5-Chloro-2-cyclohexyl-valeric acid hydrazide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N'-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate | HCID 66838991 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 5-Chloro-2-cyclohexyl-valeric acid hydrazide hydrochloride | HCID 66839453 | 229.7% |
Reaction Steps
tert-Butyl N′-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate (155 mg) was dissolved in a solution of 4 N hydrogen chloride in dioxane (2 ml), and the reaction solution was stirred at room temperature for one hour. The reaction solution was concentrated under reduced pressure to obtain 144 mg of the title compound. The property value of the compound is as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935815B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-3003b35eed6748cfa68010ac9fd15804 |
| Source note | uspto-grants-2011_05 |