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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 546699Generated: October 31, 2026

tert-butyl N'-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate → 5-Chloro-2-cyclohexyl-valeric acid hydrazide hydrochloride

https://huagongshe.com/reaction/546699

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-butyl N'-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylateHCID 66838991—
SolventHydrochloric AcidHCID 313—
Solvent1,4-DioxaneHCID 31275—
Product5-Chloro-2-cyclohexyl-valeric acid hydrazide hydrochlorideHCID 66839453229.7%

Reaction Steps

tert-Butyl N′-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate (155 mg) was dissolved in a solution of 4 N hydrogen chloride in dioxane (2 ml), and the reaction solution was stirred at room temperature for one hour. The reaction solution was concentrated under reduced pressure to obtain 144 mg of the title compound. The property value of the compound is as follows.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07935815B2
Source datasetuspto-grants-2011_05
ORD IDord-3003b35eed6748cfa68010ac9fd15804
Source noteuspto-grants-2011_05