HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66839144, compound → HCID 66839255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66839144 | HCID 66839144 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66839255 | HCID 66839255 | 212.4% |
Reaction Steps
tert-Butyl N′-[5-chloro-2-(tetrahydropyran-4-yl)-pentanoyl]-hydrazinecarboxylate (250 mg) was dissolved in a solution of 4 N hydrogen chloride in dioxane (2 ml), and the reaction solution was stirred at room temperature for 2.5 hours. The reaction solution was concentrated under reduced pressure to obtain 215 mg of the title compound. The property value of the compound is as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07935815B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-4ee3e0f2b6414d0a9f9cf38b524501ff |
| Source note | uspto-grants-2011_05 |