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HRID54690

反应详情

EQUATION

反应方程式

HRID 54690 的结构方程式

REACTANTS

反应物

2
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：Br.Br.O=C(Cn1c(NCCO)nc2ccccc21)c1ccccc1
HCID19040800

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Cn1c(NCCO)nc2ccccc21)c1ccccc1
HCID2850100

2-{2-[(2-hydroxyethyl)amino]-1H-benzimidazol-1-yl}-1-phenylethanone

C17H17N3O2

PROCEDURE

实验过程

Add 22% ammonium hydroxide to 75 ml of a hot solution of the dihydrobromide obtained in Step A in 95° alcohol until a pH of approximately 10 is obtained. The title compound precipitates and is filtered, washed with water and dried.

WORKUP

后处理

  1. customis obtained
  2. customThe title compound precipitates
  3. filtrationis filtered
  4. washwashed with water
  5. customdried