HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 3265106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 178483518 | HCID 178483518 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3265106 | HCID 3265106 | 90% |
Reaction Steps
Heat at reflux for 25 minutes 3 mmol of the hydrobromide obtained in Step A and 4 g of sodium carbonate in 25 ml of ethanol. Evaporate, treat the residue twice with 10 ml of chloroform each time, and pass the resulting chloroform solutions over a column of alumina. Evaporate the eluate. The title compound is obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05623073 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-f5081583cf91431da358561f1507debe |
| Source note | uspto-grants-1997_04 |