HRID54702

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID313

Hydrochloric Acid

ClH

结构：Cc1nc2n(CCN3CCOCC3)c3ccccc3n2c1C(=O)c1ccc(Cl)cc1

HCID12965842

未命名化合物

PRODUCTS

生成物

结构：Cc1nc2n(CCN3CCOCC3)c3ccccc3n2c1C(=O)c1ccc(Cl)cc1.Cl.Cl

HCID19040811

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

1.7 g of the base obtained in Step B is dissolved in 30 ml of acetone and acidified with concentrated hydrochloric acid: the title compound precipitate is removed by filtration and recrystallised from ethanol.

WORKUP

后处理

customthe title compound precipitate is removed by filtration
customrecrystallised from ethanol