HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67201906, compound → HCID 44193195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67201906 | HCID 67201906 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44193195 | HCID 44193195 | — |
Reaction Steps
1-{2-[1-(2-Hydroxy-ethyl)-1H-indol-3-yl]-5H-pyrrolo[2,3-b]pyrazin-7-yl}-2,2-dimethyl-propan-1-one was prepared following the same procedure but using 1-[2-{1-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-1H-indol-3-yl}-5-(2-trimethylsilanyl-ethoxymethyl)-5H-pyrrolo[2,3-b]pyrazin-7-yl]-2,2-dimethyl-propan-1-one as starting material. The product was obtained in 67% by trituration in MeOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07939531B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-e279fe62c20f4c2884e1b0fc5ad776e9 |
| Source note | uspto-grants-2011_05 |