HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22319133, compound → (6-Methoxypyridin-3-yl)(pyridin-2-yl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22319133 | HCID 22319133 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | (6-Methoxypyridin-3-yl)(pyridin-2-yl)methanone | HCID 22319071 | 97.3% |
Reaction Steps
To a solution of 0.83 g of α-(2-methoxypyridin-5-yl)-2-pyridinemethanol in 20 ml of an acetone was added 1.70 g of activated manganese dioxide, followed by vigorously stirring at room temperature for 30 minutes. The resulting precipitates were filtered off and washed with acetone. Then, the filtrate was concentrated, to give 0.80 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07939549B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-2c3d9b86e2284e49b1ee912fbb5f1ef0 |
| Source note | uspto-grants-2011_05 |