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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 54778Generated: October 25, 2026

1-Butanaminium, N,N,N-tributyl-, azide → Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester

https://huagongshe.com/reaction/54778

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Butanaminium, N,N,N-tributyl-, azideHCID 5743232—
ReactantEthanethioic acid cis-(+/-)-S-[tetrahydro-5-[[[(trifluoromethyl)-sulfonyl]oxy]methyl]-3-furanyl]esterHCID 86750330—
SolventDichloromethaneHCID 6344—
ProductEthanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]esterHCID 8675033187.8%

Reaction Steps

The title compound is prepared by the procedure of Example 43 using 0.560 g of product from Example 60 in 2 ml of methylene chloride, 0.569 g of tetrabutylammonium azide in 2 ml of methylene chloride to give 0.321 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05623081
Source datasetuspto-grants-1997_04
ORD IDord-8808e9b3904943e3bfecb2393f2ea08f
Source noteuspto-grants-1997_04