HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 4-Methoxy-3-propoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 3-Ethoxy-4-methylbenzaldehyde | HCID 25242058 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-Methoxy-3-propoxybenzaldehyde | HCID 592109 | — |
Reaction Steps
The title compound was prepared by reaction of isovanillin with propyl iodide in DMF using K2CO3 as base in analogy to the preparation of 3-ethoxy-4-methyl-benzaldehyde (intermediate B21, vide infra).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07939661B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-b7a1077f4664476b9e7e6b449dbd2fb2 |
| Source note | uspto-grants-2011_05 |