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HRID54816

反应详情

EQUATION

反应方程式

HRID 54816 的结构方程式

REACTANTS

反应物

4
结构：CCO
HCID702

Ethanol

C2H6O

结构：CC(C)[C@H](N)C(=O)O
HCID6287

L-Valine

C5H11NO2

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(OCc1ccc([N+](=O)[O-])cc1)Oc1ccc([N+](=O)[O-])cc1
HCID21829967

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)[C@H](NC(=O)OCc1ccc([N+](=O)[O-])cc1)C(=O)O
HCID54494215

N-{[(4-Nitrophenyl)methoxy]carbonyl}-L-valine

C13H16N2O6

收率 35.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 255 using 14.73 g of product from Example 254, 5.42 g of L-valine, 12.75 ml of triethylamine and 556 ml of 4:1 ethyl alcohol:water to give 4.89 g of the desired product after chromatography.